Tuesday, May 10, 2016

Testing!

I finally started testing the chemicals last week. Yay! I know I'm about a month off schedule and that the project is due in barely a week, but I made a plan last week. I've stayed on track for the past 6 days. Here is what the past 6 days have looked like:

ChemicalSpray/Soak TimeTest TimeAmount of ChemicalAmount of Water SprayedAmount of Water CollectedNotesRetest?
Control (nothing)9pm 4/26-7pm 4/277:30-8:00N/A250ml0
Sakrete9pm 4/26-7pm 4/277:25-7:55500ml250ml0Edges crumbly and green on second day
Gypsum9pm 4/26-7pm 4/278:04-8:34250ml (60ml gypsum+250ml H2O)250ml~30ml (retest needed)Retest neededYes
Alcohol and Burn7pm 4/28 (but n/a)9:41-10:11500ml250ml~20ml250ml spray then burn; 250ml spray while burning. Surface hotNo; unrealistic
Vinegar7:15pm 4/28-9pm 4/299:13-9:43250ml250ml~40mlBubbling a little after sprayed chemicalYes
Ammonia6:30pm 4/28-9pm 4/299:09-9:39250ml250ml0Poured instead of sprayed chemical
Hydrochloric Acid3:45pm 4/30-4pm 5/14:33-5:03250ml250ml~40mlFoamed up yellow/green when poured chemical; Poured because of dangerNo; unrealistic
Bleach3:30pm 4/30-4pm 5/13:59-4:29250ml250ml50mlYes; a lot of H20
Hydrogen Peroxide3:20pm 4/30-4pm 5/13:56-4:26250ml250ml~10mlGreenish square formed in center; Fizzing/bubbles when spraying chemicalNo; not enough
Sulfuric acid3:20pm 5/2-4pm 5/34:20-4:50250ml250ml15mlBubbling/fizzing when sprayed chemicalNo; unrealistic
Coke3:30pm 5/2-4pm 5/34:54-5:24250ml250ml20ml
Calcium Chloride3:15pm 5/2-4pm 5/34:23-4:53250ml250ml10mlWhite residue on concrete after 24 hoursNo; unrealistic
Seawater6pm 5/4-4:30pm 5/54:33-5:03250ml250ml0Salt residue on tub after 24 hours
Dry Ice6pm 5/4-4:30pm 5/54:30-5:005 lb250ml0All dry ice gone after 24 hours

Basically, I spray the concrete with 250ml of chemical one day and let it soak until the next day afternoon. After those ~24 hours, I put the slab on top of a bucket and spray it with 250ml of water. I let the water sit for 30 minutes, then measure how much has dripped through the concrete and into the bucket below.

There may be a few flaws in this experiment, including water seeping into the bucket from the edges of the slab and differences in amount of water actually landing on the concrete. To remedy this I will be retesting some of the highest performing materials. Here are my retest results:

ChemicalSpray/Soak TimeTest TimeAmount of ChemicalAmount of Water PouredAmount of Water CollectedNotes
Gypsum5pm 5/6-6pm 5/76:13-6:43250ml (60ml gyspum)250ml55mlUsed crayon wax as sealant; no visible drip into bucket from sides
Vinegar5pm 5/6-6pm 5/76:22-6:52250ml250ml30mlUsed candle wax as sealant; no visible drip into bucket from sides
Bleach5pm 5/6-6pm 5/76:59-7:29250ml250ml50mlUsed candle wax as sealant; no visible drip into bucket from sides

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